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Наткнулся на Аваксе: Dana W. Mayo, Ronald M. Pike and David C. Forbes, "Microscale Organic Laboratory: with Multistep and Multiscale Syntheses" Fifth Edition, Wiley 2011 | ISBN: 0471215023, ISBN 978-0-471-21502-8 (Main Book) | 704 (751) pages | PDF | 43,3 MB
This is a laboratory text for the mainstream organic chemistry course taught at both two and four year schools, featuring both microscale experiments and options for scaling up appropriate experiments for use in the macroscale lab. It provides complete coverage of organic laboratory experiments and techniques with a strong emphasis on modern laboratory instrumentation, a sharp focus on safety in the lab, excellent pre- and post-lab exercises, and multi-step experiments. Notable enhancements to this new edition include inquiry-driven experimentation, validation of the purification process, and the implementation of greener processes (including microwave use) to perform traditional experimentation.
The Refractive Index material, which was formally in chapter 4, has been moved to the book companion web site: http://www.wiley.com/college/mayo.
Chapter 10W, “Advanced Microscale Organic Laboratory Experiments,” (formerly chapter 7) has been moved to the book companion web site: http://www.wiley.com/college/mayo.
These web reference discussions include information on the following topics:
• Microscale lab equipment and techniques
• Semimicroscale distillation
• Reduced pressure distillations with microspinning band columns
• Vacuum pumps and pressure regulation
• Crystallization
The Instructor’s Manual, also available on the web site, provides a list of chemicals for each experiment, setup suggestions, and anticipated outcomes.
• Measurement of Specific Rotation
• Introduction to Infrared Spectroscopy—Introduction to Theory
• Group Frequencies of the Hydrocarbons
• Characteristic Frequencies of the Heteroatom Functional Groups
• Instrumentation—the Infrared Interferometer
• Tables of DerivativesMicroscaleOrganicLaboratory5ed2011Mayo%26amp%3B.rar 10.75 MB
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