Hiroaki Egawa, , Etsuo Yonemochi and Katsuhide Terada
Investigation of optimal manufacturing process for freeze-dried formulations: Observation of frozen solutions by low temperature X-ray diffraction measurements
Thermochimica Acta Volume 431, Issues 1-2, 15 June 2005, Pages 127-132
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http://dx.doi.org/10.1016/j.tca.2005.01.057