Доклады АН СССР, 1962 - Гесс, Ol.Lo, спасибо!

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В. С. Этлис, Г. А. Разуваев.
ДАН СССР, 1962, 143, c.633.
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[Гесс]

Согласно скайфу Reaction of 3-aminopropene 1,2-thiocarbonate with ammonia and amines

cf. CA 57, 656e. Heating I with 3 moles NH3 in EtOH 8-​10 hrs. at 120-​30° gave 61​% II, b6 75-​6°, n20D 1.5415, d20 1.2170; α-​naphthylurethan m. 165-​6°. Similarly, alc. Me2NH at 140-​50° gave Me2NCONH2 and II. Heating thioepichlorohydrin with KOAc in AcOH 1 hr. at 110° gave 55​% II acetate, b9 72-​3°, 1.4880, 1.1784, which hydrolyzed to give 81​% II, b5 70-​1°, 1.5415, 1.2155, on heating with alc. KOH 1 hr. Epichlorohydrin and NaSH in EtOH also gave II in low yield. It was suggested that II was prepd. but not recognized by previous workers (Beilstein, Handbuch der Organischen Chemic 4th ed. 17, 106(1933)​)​.

[Ol.Lo]

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