+++ ищю статью из Chem.Abstr., 1969, vol. 70, # 37338n.

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Chem.Abstr., 1969, vol. 70, # 37338n.

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Condensation of benzaldehyde and m-nitrobenzaldehyde with nitromethane in liquid ammonia. II
By: Rumyantsev, N. P.; Rumyantseva, K. S.; Lopatina, E. A.
Uchenye Zapiski - Mordovskii Gosudarstvennyi Universitet (1967), No. 60, 49-53 | Language: Russian, Database: CAplus
The reaction of MeNO2 with BzH or m-O2NC6H4CHO (I) in liquid NH3 was studied. To the solution of 1.3 cc. MeNO2 in 150 cc. liquid NH3 1.8 cc. BzH was added. After 8-10 hrs., liquid NH3 was evaporated and 15% [PhCH(OH)]3CNO2 m. 155-7° (Me2CO-EtOH) was obtained. To the 150 cc. liquid NH3, 3 cc. MeNO2 and 0.7 cc. I was added dropwise to give 82% m-O2NC6H4CH(OH)CH2-NO2, 71-1.5° (C6H6-EtOH).

Keywords: benzaldehyde nitromethane; condensations benzaldehyde nitrobenzaldehyde; nitrobenzaldehyde condensations benzaldehyde; hydroxy benzyl nitromethanes; benzyl nitromethanes hydroxy; nitromethanes hydroxy benzyl

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